Invention Grant
- Patent Title: Modulating microstructure in interconnects
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Application No.: US14965991Application Date: 2015-12-11
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Publication No.: US09721835B2Publication Date: 2017-08-01
- Inventor: Daniel C. Edelstein , Chih-Chao Yang
- Applicant: International Business Machines Corporation
- Applicant Address: US NY Armonk
- Assignee: INTERNATIONAL BUSINESS MACHINES CORPORATION
- Current Assignee: INTERNATIONAL BUSINESS MACHINES CORPORATION
- Current Assignee Address: US NY Armonk
- Agency: Cantor Colburn LLP
- Agent Steven Meyers
- Main IPC: H01L21/768
- IPC: H01L21/768

Abstract:
Recrystallization and grain growth of an interconnect metal, such as Cu, is achieved at higher anneal temperatures of 150° C. to 600° C., for example, for short anneal times of five to 180 minutes by forming a metal stress locking layer on the interconnect metal before anneal and chemical-mechanical polishing. The stress locking layer extends the elastic region of the interconnect metal by suppressing atom diffusion to the free surface, resulting in near zero tensile stress at room temperature after anneal. Stress voiding, which creates reliability problems, is thereby avoided. Improved grain size and texture are also achieved. The stress locking layer is removed after anneal by chemical-mechanical polishing or wet etching leaving the metal interconnect with low stress and improved grain size and texture. Annealing can be done in a forming gas or nitrogen gas atmosphere.
Public/Granted literature
- US20170170063A1 MODULATING MICROSTRUCTURE IN INTERCONNECTS Public/Granted day:2017-06-15
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