Invention Grant
- Patent Title: Device and method for re-circulating raw material used when manufacturing polybutene
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Application No.: US14908702Application Date: 2014-07-29
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Publication No.: US09637576B2Publication Date: 2017-05-02
- Inventor: Myeong Seok Kim , Min Sup Park , Kyoung Tae Min
- Applicant: DAELIM INDUSTRIAL CO., LTD.
- Applicant Address: KR Seoul
- Assignee: DAELIM INDUSTRIAL CO., LTD.
- Current Assignee: DAELIM INDUSTRIAL CO., LTD.
- Current Assignee Address: KR Seoul
- Agency: Nath, Goldberg & Meyer
- Agent Jerald L. Meyer; Tanya E. Harkins
- Priority: KR10-2013-0090023 20130730
- International Application: PCT/KR2014/006933 WO 20140729
- International Announcement: WO2015/016577 WO 20150205
- Main IPC: C08F2/00
- IPC: C08F2/00 ; B01J19/00 ; C08F110/08 ; C08F6/02 ; C08J11/02 ; B01J19/24

Abstract:
Disclosed are a device and a method for continuously polymerizing polybutene by removing halogen acid, which is included in a reaction raw material, by adsorbing the halogen acid using an adsorbent and then re-supplying the reaction raw material into a reactor. The device for re-circulating the raw material when manufacturing polybutene comprises a reactor, into which a catalyst and a reaction raw material (diluted with an inactive organic solvent) are supplied and polymerized to produce a reaction product; a neutralizing/washing tank for removing the catalyst from the reaction product and neutralizing the reaction product; a separation tank for separating the reaction product into organic compounds and water; a C4 distillation column for distilling an unreacted raw material and the inactive organic solvent from the organic compounds; and an impurity adsorption column for removing halogen acid from the distilled unreacted raw material and the inactive organic solvent using an adsorbent.
Public/Granted literature
- US20160176994A1 DEVICE AND METHOD FOR RE-CIRCULATING RAW MATERIAL USED WHEN MANUFACTURING POLYBUTENE Public/Granted day:2016-06-23
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