Invention Grant
- Patent Title: Method for recovering ethylene during the process for producing VAC and a device thereof
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Application No.: US14356602Application Date: 2012-11-06
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Publication No.: US09636627B2Publication Date: 2017-05-02
- Inventor: Minhua Zhang , Xiuqin Dong , Cheng Liu , Minli Tao , Yonghui Li , Huisheng Lv , Yingzhe Yu , Zhongfeng Geng
- Applicant: Yingjin Yuan
- Applicant Address: CN Tianjin
- Assignee: Tianjin University
- Current Assignee: Tianjin University
- Current Assignee Address: CN Tianjin
- Agency: Bei & Ocean
- Agent George G. Wang
- Priority: CN201110357506 20111111
- International Application: PCT/CN2012/084164 WO 20121106
- International Announcement: WO2013/067918 WO 20130516
- Main IPC: B01D53/18
- IPC: B01D53/18 ; B01D53/14 ; C07C7/11

Abstract:
The present invention discloses a method and a device for recovering ethylene during the process for producing vinyl acetate, wherein a double solvent absorption method composed of an absorbent solution and deionized water is adopted. The method is as follows: introducing an outlet stream as an absorbent solution from the upper section of the feeding plate in an acetic acid tower during the rectification stage of vinyl acetate production; delivering same to the top of the lower section of the ethylene recovery tower by a delivery pump; charging refined gas from the tower bottom of the ethylene recovery tower for contacting with the absorbent solution in a counter-current; delivering the absorption bottom solution to the rectification stage for treatment; the gas continuing to rise to the upper section of the ethylene recovery tower and contacting with the deionized water introduced from the top of the tower in a counter-current; absorbing and removing the acetic acid therein; and discharging the residual inert gas, such as N2, from the top of the ethylene recovery tower. The absorbent solution is a mixture of acetic acid, vinyl acetate and water, and comprises by weight percentage of 50-85% acetic acid, 5-30% vinyl acetate and 5-20% water.
Public/Granted literature
- US20140366729A1 Method for Recovering Ethylene during the Process for Producing VAC and a Device thereof Public/Granted day:2014-12-18
Information query
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