Invention Grant
- Patent Title: Method for producing aqueous ethylene/vinyl alcohol based copolymer dispersion
- Patent Title (中): 乙烯/乙烯醇系共聚物分散液的制造方法
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Application No.: US11596355Application Date: 2005-05-13
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Publication No.: US08664313B2Publication Date: 2014-03-04
- Inventor: Norihiro Sugihara , Yuhei Funabiki
- Applicant: Norihiro Sugihara , Yuhei Funabiki
- Applicant Address: JP Hyogo
- Assignee: Sumitomo Seika Chemicals Co., Ltd.
- Current Assignee: Sumitomo Seika Chemicals Co., Ltd.
- Current Assignee Address: JP Hyogo
- Agency: Novak Druce Connolly Bove + Quigg LLP
- Priority: JP2004-145410 20040514
- International Application: PCT/JP2005/008784 WO 20050513
- International Announcement: WO2005/111118 WO 20051124
- Main IPC: C08K5/05
- IPC: C08K5/05 ; C08L29/04 ; C08F6/10

Abstract:
The present invention provides a method of producing, in an industrially advantageous manner, an ethylene/vinyl alcohol copolymer aqueous dispersion which has a high concentration and is excellent in long-term storage stability and in which the resin particles in the aqueous dispersion obtained are small in particle diameter. The method of the present invention relates to producing an ethylene/vinyl alcohol copolymer aqueous dispersion, which comprises: (1) a step of dissolving an ethylene/vinyl alcohol copolymer in a mixed solvent comprising 5 to 65% by weight of water and 35 to 95% by weight of a water-soluble organic solvent, with heating, (2) a step of cooling a solution obtained in step (1) to precipitate the ethylene/vinyl alcohol copolymer, (3) a step of reducing a concentration of the water-soluble organic solvent in the mixed solvent to a level lower than 35% by weight relative to the total amount of the water and water-soluble organic solvent by adding water, and (4) a step of distilling off the water-soluble organic solvent.
Public/Granted literature
- US20080176989A1 Method For Producing Aqueous Ethylene/Vinyl Alcohol Based Copolymer Dispersion Public/Granted day:2008-07-24
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