Invention Grant
- Patent Title: Purification of aqueous solutions of organic acids
- Patent Title (中): 纯化有机酸水溶液
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Application No.: US12973775Application Date: 2010-12-20
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Publication No.: US08192589B2Publication Date: 2012-06-05
- Inventor: Hendrik Martinus Winkelaar , Jan Van Breugel , Margarita Camprubi Vilá , José Maria Vidal Lancis
- Applicant: Hendrik Martinus Winkelaar , Jan Van Breugel , Margarita Camprubi Vilá , José Maria Vidal Lancis
- Applicant Address: NL Gorinchem
- Assignee: Purac Biochem B.V.
- Current Assignee: Purac Biochem B.V.
- Current Assignee Address: NL Gorinchem
- Agency: Foley & Lardner LLP
- Agent Gilberto M. Villacorta; Sunit Talapatra
- Priority: NL1013682 19991126
- Main IPC: B01D1/22
- IPC: B01D1/22 ; B01D3/10 ; B01D3/28 ; C07C51/44

Abstract:
The invention relates to a method and a device for the purification of an aqueous solution of an organic acid having a boiling point at atmospheric pressure of less than 450° C., which further has approximately 275 g carboxylate ions/l or less, preferably 250 g carboxylate ions/l or less, and preferably less than 1% by weight ionic impurities, calculated on the basis of the total solution. In particular, the invention relates to a method and a device for the continuous purification and concentration, on an industrial scale, of an aqueous solution of an organic acid having a boiling point at atmospheric pressure of less than 450° C. According to the method, this solution is subjected to two or more distillation steps, the first distillation step being carried out at a temperature of from 80° to 150° C. and a pressure of from 50 to 250 mbar, and the second distillation step being carried out at a temperature of from 80° to 200° C. and a pressure of from 0.01 to 50 mbar.
Public/Granted literature
- US20110089016A1 PURIFICATION OF AQUEOUS SOLUTIONS OF ORGANIC ACIDS Public/Granted day:2011-04-21
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