Invention Grant
US08128758B2 R-Fe-B microcrystalline high-density magnet and process for production thereof
有权
R-Fe-B微晶高密度磁铁及其制造方法
- Patent Title: R-Fe-B microcrystalline high-density magnet and process for production thereof
- Patent Title (中): R-Fe-B微晶高密度磁铁及其制造方法
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Application No.: US12254967Application Date: 2008-10-21
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Publication No.: US08128758B2Publication Date: 2012-03-06
- Inventor: Noriyuki Nozawa , Takeshi Nishiuchi , Satoshi Hirosawa , Tomohito Maki
- Applicant: Noriyuki Nozawa , Takeshi Nishiuchi , Satoshi Hirosawa , Tomohito Maki
- Applicant Address: JP Tokyo
- Assignee: Hitachi Metals, Ltd.
- Current Assignee: Hitachi Metals, Ltd.
- Current Assignee Address: JP Tokyo
- Agency: Keating & Bennett, LLP
- Priority: JP2006-324298 20061130; JP2007-116661 20070426
- Main IPC: H01F1/057
- IPC: H01F1/057

Abstract:
An R—Fe—B based rare-earth alloy powder with a mean particle size of less than about 20 μm is provided and compacted to make a powder compact. Next, the powder compact is subjected to a heat treatment at a temperature of about 550° C. to less than about 1,000° C. within hydrogen gas, thereby producing hydrogenation and disproportionation reactions (HD processes). Then, the powder compact is subjected to another heat treatment at a temperature of about 550° C. to less than about 1,000° C. within either a vacuum or an inert atmosphere, thereby producing desorption and recombination reactions and obtaining a porous material including fine crystal grains, of which the density is about 60% to about 90% of their true density and which have an average crystal grain size of about 0.01 μm to about 2 μm (DR processes). Thereafter, the porous material is subjected to yet another heat treatment at a temperature of about 750° C. to less than about 1,000° C. within either the vacuum or the inert atmosphere, thereby further increasing its density to about 93% or more of their true density and making an R—Fe—B based microcrystalline high-density magnet.
Public/Granted literature
- US20090032147A1 R-Fe-B MICROCRYSTALLINE HIGH-DENSITY MAGNET AND PROCESS FOR PRODUCTION THEREOF Public/Granted day:2009-02-05
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