Invention Grant
US07671244B2 Method for producing 1,2-dichloroethane by means of direct chlorination
有权
通过直接氯化生产1,2-二氯乙烷的方法
- Patent Title: Method for producing 1,2-dichloroethane by means of direct chlorination
- Patent Title (中): 通过直接氯化生产1,2-二氯乙烷的方法
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Application No.: US11793882Application Date: 2005-12-15
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Publication No.: US07671244B2Publication Date: 2010-03-02
- Inventor: Harald Hafenscher , Reinhold Weis , Michael Benje
- Applicant: Harald Hafenscher , Reinhold Weis , Michael Benje
- Applicant Address: DE Dortmund
- Assignee: UHDE GmbH
- Current Assignee: UHDE GmbH
- Current Assignee Address: DE Dortmund
- Agency: Marshall & Melhorn, LLC
- Priority: DE102004063090 20041222
- International Application: PCT/EP2005/013535 WO 20051215
- International Announcement: WO2006/069640 WO 20060706
- Main IPC: C07C17/02
- IPC: C07C17/02 ; C07C17/093

Abstract:
The invention relates to a method for producing high-purity 1,2-dichloroethane from dissolved chlorine and dissolved ethylene which are brought into contact with each other using a circulating liquid reaction medium which essentially consists of 1,2-dichloroethane and a catalyst and passes through at least one reaction loop. The two limbs of the loop are connected to a gas-phase stripping container which is arranged at the top and from which the reaction product is outwardly transferred either in a gaseous or liquid form or both in a gaseous form and in a liquid form. The addition points for the addition of chlorine and dissolved ethylene are arranged in the limb of the loop in which the liquid rises. The addition point for dissolved chlorine is always arranged downstream of the ethylene addition point. At least one addition point for liquid 1,2-dichloroethane follows each chlorine addition point, and the addition of the liquid 1,2-dichloroethane is carried out under kinetic energy which is high enough to enable a vigorous mixture of 1,2-dichloroethane, dissolved chlorine and ethylene to be carried out. Preferably, the liquid 1,2-dichloroethane is added by means of at least one jet mixer.
Public/Granted literature
- US20080146854A1 Method for Producing 1,2-Dichloroethane by Means of Direct Chlorination Public/Granted day:2008-06-19
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