- Patent Title: Die and piston of an SPS apparatus, SPS apparatus comprising same, and method of sintering, densification or assembly in an oxidising atmosphere using said apparatus
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Application No.: US15772219Application Date: 2016-11-03
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Publication No.: US11642724B2Publication Date: 2023-05-09
- Inventor: Alexandre Allemand , Alain Largeteau , Seu U-Chan Chung , Yann Le Petitcorps , Jérôme Roger
- Applicant: COMMISSARIAT A L'ENERGIE ATOMIQUE ET AUX ENERGIES ALTERNATIVES , CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE
- Applicant Address: FR Paris
- Assignee: COMMISSARIAT A L'ENERGIE ATOMIQUE ET AUX ENERGIES ALTERNATIVES,CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE
- Current Assignee: COMMISSARIAT A L'ENERGIE ATOMIQUE ET AUX ENERGIES ALTERNATIVES,CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE
- Current Assignee Address: FR Paris; FR Paris
- Agency: Pearne & Gordon LLP
- Priority: FR 60561 2015.11.04
- International Application: PCT/EP2016/076555 2016.11.03
- International Announcement: WO2017/076971A 2017.05.11
- Date entered country: 2018-04-30
- Main IPC: B22F3/105
- IPC: B22F3/105 ; C04B35/111 ; C23C16/32 ; C04B35/01 ; C04B35/46 ; C04B35/468 ; B28B3/02 ; B22F3/11 ; C04B35/115 ; C04B35/457 ; C04B35/486 ; C04B35/645 ; H05B3/60

Abstract:
A die or piston of a spark plasma sintering apparatus, wherein the die or piston is made from graphite and the outer surfaces of the die or piston are coated with a silicon carbide layer with a thickness of 1 to 10 micrometres, the silicon carbide layer being further optionally coated with one or more other layer(s) made from a carbide other than silicon carbide chosen from hafnium carbide, tantalum carbide and titanium carbide, the other layer(s) each having a thickness of 1 to 10 micrometres. A spark plasma sintering (SPS) apparatus comprising the die and two of the pistons, defining a sintering, densification or assembly chamber capable of receiving a powder to be sintered, a part to be densified, or parts to be assembled. A method of sintering a powder, densifying a part, or assembling two parts by means of a method of spark plasma sintering (SPS) in an oxidising atmosphere, using the spark plasma sintering (SPS) apparatus.
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